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Product Details
Synthesis Reference(s) |
Journal of the American Chemical Society, 63, p. 3452, 1941 DOI: 10.1021/ja01857a057Tetrahedron Letters, 33, p. 7535, 1992 DOI: 10.1016/S0040-4039(00)60817-1 |
InChI:InChI=1/C18H15NO2/c1-2-21-18(20)16(13-19)17(14-9-5-3-6-10-14)15-11-7-4-8-12-15/h3-12H,2H2,1H3
Octocrylene is an organic UV filter, com...
The invention provides a preparation met...
The invention provides a preparation met...
The invention discloses a preparation me...
A variety of functionalized coumarins we...
benzophenone
ethyl 2-cyanoacetate
etocrylene
Conditions | Yield |
---|---|
With ammonium acetate; pyrographite; In n-heptane; for 15h; Ionic liquid; Reflux;
|
94.1% |
With acetic acid; 3-amino propanoic acid; In benzene; for 90h; Heating;
|
64% |
|
|
With ammonium acetate; acetic acid; benzene;
|
|
With ammonium acetate; acetic acid; In n-heptane; for 24h; Reflux;
|
|
With ammonium acetate; acetic acid; at 45 - 72 ℃; for 10h; Reagent/catalyst;
|
Benzophenone imine
ethyl 2-cyanoacetate
etocrylene
Conditions | Yield |
---|---|
In methanol; at 35 - 85 ℃; Inert atmosphere;
|
96% |
|
benzophenone
ammonium acetate
acetic acid
ethyl 2-cyanoacetate
2-cyano-3,3-diphenylacrylic acid
ethyl α-cyano-ββ-diphenylpropionate
2-benzhydrylidene-malonamic acid
(+/-)-2-Aethyl-2,3-dicyan-3,3-diphenyl-propionsaeure-aethylester
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