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The invention provides a preparation met...
The invention relates to an alpha-hydrox...
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The invention discloses a cheap and effi...
1-(4-(2-hydroxyethoxy)phenyl)-2-methylpropan-1-one
![(2-hydroxy-1-[4-(2-hydroxyethoxy)phenyl]-2-methyl-1-propanone)](/upload/2024/10/821e159d-3636-4022-a210-33a335f3bd0d.png)
(2-hydroxy-1-[4-(2-hydroxyethoxy)phenyl]-2-methyl-1-propanone)
| Conditions | Yield |
|---|---|
|
With
N-Bromosuccinimide; dimethyl sulfoxide;
at 100 ℃;
for 24h;
|
92% |
|
With
N-Bromosuccinimide; dimethyl sulfoxide;
at 60 ℃;
for 24h;
Schlenk technique;
|
92% |
|
With
oxygen; caesium carbonate; triethyl phosphite;
In
dimethyl sulfoxide;
at 25 ℃;
for 24h;
under 760.051 Torr;
Schlenk technique;
|
75% |
|
With
dihydrogen peroxide;
In
dichloromethane;
at 30 ℃;
Microwave irradiation;
|
71% |
4-hydroxyethyltrichloromethylbenzene
cyclohexanone
(2-hydroxy-1-[4-(2-hydroxyethoxy)phenyl]-2-methyl-1-propanone)
| Conditions | Yield |
|---|---|
|
With
magnesium;
In
N,N-dimethyl-formamide;
at -20 - -10 ℃;
for 2h;
Inert atmosphere;
|
78% |
4-(2-acetoxyethoxy)-phenyl 2-propyl ketone
1-(4-(2-hydroxyethoxy)phenyl)-2-methylpropan-1-one
2-phenoxyethyl acetate
cyclohexanone
2-[4-(2-hydroxy-2-methylpropanoyl)phenoxy]ethyl prop-2-enoate
4-(2-acryloyloxyethoxy)-phenyl 2-acryloyloxy-2-propyl ketone
2-Hydroxy-2-methyl-1-[4-(2-oxiranylmethoxyethoxy)phenyl]propan-1-one
C16H20O6
CAS：86428-83-3
CAS：29049-45-4
CAS：2092357-48-5
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