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InChI:InChI=1/C26H27O3P/c1-16-12-18(3)23(19(4)13-16)25(27)30(29,22-10-8-7-9-11-22)26(28)24-20(5)14-17(2)15-21(24)6/h7-15H,1-6H3
A straightforward high-yield synthesis f...
The invention provides a preparation met...
The invention relates to the field of ne...
The invention provides a preparation met...
The invention relates to the field of ph...
Dichlorophenylphosphine
chloro-diphenylphosphine
mesitylene-2-carboxylic acid chloride
phenyl bis(2,4,6-trimethylbenzoyl)phosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
| Conditions | Yield |
|---|---|
|
Dichlorophenylphosphine; chloro-diphenylphosphine; mesitylene-2-carboxylic acid chloride;
With
zinc;
In
ethyl acetate;
at 20 ℃;
for 6h;
Inert atmosphere;
Large scale;
With
water; dihydrogen peroxide;
In
ethyl acetate;
for 0.5h;
Reagent/catalyst;
Solvent;
Inert atmosphere;
Large scale;
|
23.1 kg 18.7 kg |
Dichlorophenylphosphine
chloro-diphenylphosphine
mesitylene-2-carboxylic acid chloride
phenyl bis(2,4,6-trimethylbenzoyl)phosphine oxide
phenyl(2,4,6-trimethylbenzoyl)phosphinic acid
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
| Conditions | Yield |
|---|---|
|
Dichlorophenylphosphine; chloro-diphenylphosphine; mesitylene-2-carboxylic acid chloride;
With
zinc;
In
ethyl acetate;
at 20 ℃;
for 2h;
Inert atmosphere;
With
water; dihydrogen peroxide;
In
ethyl acetate;
for 0.5h;
Inert atmosphere;
|
2 g 0.8 g 1.6 g |
mesitylene-2-carboxylic acid chloride
bis-(2,4,6-trimethylbenzoyl)-phenylphosphine
P,P-dichlorophenylphosphine oxide
Dichlorophenylphosphine
mesytaldehyde
4-Oxo-4-<2,4,6-trimethyl-phenyl>-but-2-ensaeure-butylester
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