83-56-7

  • Product Name1,5-Dihydroxy naphthalene
  • Molecular FormulaC10H8O2
  • Molecular Weight160.172
  • Purity99%
  • Appearancegray powder
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Product Details

Quick Details

  • CasNo: 83-56-7
  • Molecular Formula: C10H8O2
  • Appearance: gray powder
  • Purity: 99%

Chinese factory supply 1,5-Dihydroxy naphthalene 83-56-7 in stock with high standard

  • Molecular Formula:C10H8O2
  • Molecular Weight:160.172
  • Appearance/Colour:gray powder 
  • Vapor Pressure:3.62E-06mmHg at 25°C 
  • Melting Point:259-261 °C (dec.)(lit.) 
  • Refractive Index:1.725 
  • Boiling Point:375.4 °C at 760 mmHg 
  • PKA:9.28±0.40(Predicted) 
  • Flash Point:193.5 °C 
  • PSA:40.46000 
  • Density:1.33 g/cm3 
  • LogP:2.25100 

1,5-Dihydroxy naphthalene(Cas 83-56-7) Usage

Purification Methods

The diol (~30g) is purified by making into a thick paste with H2O and suspending this in 3L of H2O containing 200mL of EtOH, boiling under reflux for 3hours, cooling to 30o, saturating with SO2, digesting below the boiling point for 1hour and filtering fast through a large hot filter paper. The hot filtrate is poured onto crushed ice whereby the diol (15-20g) separates as colourless needles (m 258o) [Wheeler & Ergle J Am Chem Soc 52 4873 1930]. Recrystallise it from H2O or nitromethane under N2 to avoid oxidation. The dibenzoyl derivative has m 245o (from EtOH). The 5-methoxy-1-naphthol derivative [prepared from the diol in MeOH/HCl (1:30 weight to volume ratio) and set aside at 25o for 9-10days] crystallised from pet ether (m 135-136o) or from CH2Cl2/hexane (needles m 140o) [Bell & McCaffrey Aust J Chem 46 731 1993]. [Beilstein 6 I 477, 6 II 950, 6 III 5265, 6 IV 6554.]

InChI:InChI=1/C10H8O2/c11-9-5-1-3-7-8(9)4-2-6-10(7)12/h1-6,11-12H

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83-56-7 Process route

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Conditions
Conditions Yield
at 220 - 300 ℃; im Autoklaven;
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Conditions
Conditions Yield
With dihydrogen peroxide; pH=3; Reagent/catalyst; Concentration; pH-value; Kinetics;

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