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Product Details
General Description |
1-Bromo-3,5-dichlorobenzene on treatment with iPrMgCl.LiCl in THF and then DMF at 0°C, followed by the reaction with molecular iodine and aq NH3 yields the corresponding aromatic nitrile. |
InChI:InChI=1/C6H3BrCl2/c7-4-1-5(8)3-6(9)2-4/h1-3H
The present invention relates to an impr...
An efficient method was developed to syn...
Highly effective embodiment of Sandmeyer...
An efficient catalyst system for Sandmey...
3,5-Dichloroaniline
1-bromo-3,5-dichlorobenzene
Conditions | Yield |
---|---|
3,5-Dichloroaniline;
With
hydrogen bromide; sodium nitrite;
In
water; acetonitrile;
at 0 - 35 ℃;
With
hydrogen bromide; copper(I) bromide;
In
water; acetonitrile;
at 0 - 75 ℃;
|
72% |
(3,5-dichlorophenyl)hydrazine hydrochloride
1-bromo-3,5-dichlorobenzene
Conditions | Yield |
---|---|
With
boron tribromide; dimethyl sulfoxide;
at 80 ℃;
for 1h;
|
97% |
ethanol
2,4-dichloro-6-bromoaniline
1.4-Dibrom-2.6-dichlor-benzol
5-bromo-1,3-dichloro-2-iodobenzene
1-bromo-3,5-dichloro-2,4-dinitro-benzene
(3,5-dichlorophenyl)phenylamine
3,5,3',5'-Tetrachlor-diphenylamin
(3,5-dichloro-phenyl)-(3,5-dimethyl-phenyl)-amine
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