4477-28-5

  • Product Name4-Diazodiphenylamine sulfate
  • Molecular FormulaC12H10N3.HSO4
  • Molecular Weight293.303
  • Purity99%
Inquiry

Product Details

Quick Details

  • CasNo: 4477-28-5
  • Molecular Formula: C12H10N3.HSO4
  • Purity: 99%

Excellent chemical plant bulk supply 4-Diazodiphenylamine sulfate 4477-28-5

  • Molecular Formula:C12H10N3*HO4S
  • Molecular Weight:293.303
  • Vapor Pressure:0Pa at 25℃ 
  • Boiling Point:623.17℃[at 101 325 Pa] 
  • PSA:45.82000 
  • Density:1.512[at 20℃] 
  • LogP:2.68730 

4-Diazodiphenylamine sulfate(Cas 4477-28-5) Usage

Description

4-Diazodiphenylamine sulfate, also known as Variamine Blue RT Salt, is a chemical used as an intermediate in the screen printing industry.

Purification Methods

Dissolve 10g of the dye in 100mL of hot water. Sodium dithionite (0.4g) is then added, followed by active carbon (1.5g) and is filtered hot. To the colourless or slightly yellow filtrate a solution of saturated NaCl is added, and the mixture is cooled. The needles are filtered off, washed with cold water, dried at room temperature, and stored in a dark bottle (light sensitive). [Anderson & Steedly J Am Chem Soc 76 5144 1954, Erdey Chem Analyst 48 106 1959, Beilstein 16 H 602, 16 I 371, 16 II 307, 16 III 575. ]

  4-Diazodiphenylamine sulfate was used as an intermediate in the screen printing industry.

InChI:InChI=1/C12H10N3.H2O4S/c13-15-12-8-6-11(7-9-12)14-10-4-2-1-3-5-10;1-5(2,3)4/h1-9,14H;(H2,1,2,3,4)/q+1;/p-1

4477-28-5 Relevant articles

Synthesizing method for diazonium monomer 4-diazo diphenylamine disulfate

-

Paragraph 0020, (2016/10/10)

The invention discloses a synthesizing m...

4477-28-5 Process route

N-phenylphenylene-1,4-diamine
101-54-2

N-phenylphenylene-1,4-diamine

diphenylamine-4-diazonium hydrosulfate
4477-28-5

diphenylamine-4-diazonium hydrosulfate

Conditions
Conditions Yield
N-phenylphenylene-1,4-diamine; With hydrogenchloride; water; sodium nitrite; In ethanol; at 0 - 5 ℃; for 3h;
With sulfuric acid; at 5 - 10 ℃; for 2.5h;
64.6%
para-aminodiphenylamine sulfate
71005-33-9

para-aminodiphenylamine sulfate

diphenylamine-4-diazonium hydrosulfate
4477-28-5

diphenylamine-4-diazonium hydrosulfate

Conditions
Conditions Yield
With sodium nitrite; In water; at 5 ℃; for 10h;
 

4477-28-5 Upstream products

  • 156-10-5
    156-10-5

    p-nitrosodiphenylamine

  • 101-54-2
    101-54-2

    N-phenylphenylene-1,4-diamine

  • 71005-33-9
    71005-33-9

    para-aminodiphenylamine sulfate

4477-28-5 Downstream products

  • 3071-90-7
    3071-90-7

    1-(4-Anilino-phenylazo)-[2]naphthol

;
*Product Name
CasNo
Quantity
Company Name
Phone
*Email
*Description
*Code
Items marked with * are mandatory
Submit