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Product Details
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General Description |
4-Isopropylbenzenethiol is an aromatic thiol. It undergoes oxidation in the presence of activated carbon and xylene to afford the corresponding disulfide. 4-Isopropylbenzenethiol reacts with 2-chloro-3-formylquinolines and NaH in DMSO to afford the corresponding 2-(4-isopropylphenylthio)quinoline-3-carbaldehyde. |
InChI:InChI=1/C9H12S/c1-7(2)8-3-5-9(10)6-4-8/h3-7,10H,1-2H3/p-1
The invention provides a preparation met...
An efficient and convenient method for t...
The ring inversion barrier for thianthre...
O- and S-2-tetrahydrothienyl and 2-tetra...
4-isopropylbenzenesulfonyl chloride
4-mercapto-cumene
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride; sodium sulfide; iron; triphenylphosphine;
In
water; toluene;
at 40 ℃;
for 1h;
Reagent/catalyst;
Temperature;
|
95.8% |
|
With
triphenylphosphine;
In
toluene;
for 0.166667h;
chemoselective reaction;
Inert atmosphere;
|
78% |
|
With
phosphorus; iodine;
In
acetic acid;
Heating;
|
|
|
With
sulfuric acid; zinc;
for 5h;
Yield given;
Heating;
|
|
|
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 3h;
Heating;
|
Isopropylbenzene
4-mercapto-cumene
| Conditions | Yield |
|---|---|
|
With
chlorosulphuric acid; chloroform;
at 0 ℃;
Behandlung des Reaktionsprodukts mit Zink-Pulver und wss. H2SO4, anfangs bei 0grad, zuletzt bei Siedetemperatur;
|
|
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Multistep reaction;
|
Isopropylbenzene
4-isopropylbenzenesulfonyl chloride
Thiocarbonic acid S-(4-isopropyl-phenyl) ester O-methyl ester
((E)-1,2-dichloro-vinyl)-(4-isopropyl-phenyl)-sulfide
(p-Isopropyl-phenylmercapto)-acetaldehyd-diethylacetal
5-chloro-2-(4-isopropylfenylthio)acetophenone
5-chloro-2-(4-isopropylphenylthio)benzoic acid
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