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Product Details
An object of the present invention is to...
A monosulfonium salt in which very littl...
It is an object of the invention to prov...
The photolysis of triphenylsulfonium, tr...
diphenyl sulfide
1,1'-sulfinylbisbenzene
4-thiophenoxyphenyl(diphenyl)sulfonium hexafluoroantimonate
| Conditions | Yield |
|---|---|
|
With
potassium hexafluoroantimonate; sulfuric acid; acetic anhydride;
In
acetonitrile;
at 45 ℃;
for 1h;
Product distribution / selectivity;
|
98% |
|
With
hydrogen fluoride; antimony pentafluoride; acetic acid;
In
diethyl ether;
at 5 - 35 ℃;
for 1.5h;
Product distribution / selectivity;
|
95% |
diphenyl sulfide
1,1'-sulfinylbisbenzene
thiodi-p-phenylenebis(diphenylsulfonium) bishexafluoroantimonate
4-thiophenoxyphenyl(diphenyl)sulfonium hexafluoroantimonate
| Conditions | Yield |
|---|---|
|
With
potassium hexafluoroantimonate; sulfuric acid; acetic acid;
In
water;
for 0.5h;
diphenyl sulfide; 1,1'-sulfinylbisbenzene;
With
acetic anhydride;
In
water;
at 20 - 75 ℃;
for 1.5h;
Product distribution / selectivity;
|
|
|
With
sodium hexafluoroantimonate; sulfuric acid; acetic anhydride;
In
acetonitrile;
at 20 - 40 ℃;
for 2h;
Product distribution / selectivity;
|
|
|
With
potassium hexafluoroantimonate; sulfuric acid; acetic anhydride;
In
acetonitrile;
at 20 - 40 ℃;
for 2h;
Product distribution / selectivity;
|
1,4-bis(phenylthio)benzene
diphenyl sulfide
1,1'-sulfinylbisbenzene
CAS：75482-18-7
CAS：60565-88-0
CAS：19752-55-7
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